3-PHENOXY PROPANOIC ACID METHYL ESTER

Base Information

• Chemical Name: 3-PHENOXY PROPANOIC ACID METHYL ESTER
• CAS No.: 7497-89-4
• Molecular Formula: C10H12 O3
• Molecular Weight: 180.203
• Mol file: 7497-89-4.mol

Synonyms:Propionicacid, 3-phenoxy-, methyl ester (6CI,7CI,8CI); 3-Phenoxypropionic acid methylester; Methyl 3-phenoxypropanoate; Methyl 3-phenoxypropionate; NSC 406851

Chemical Property of 3-PHENOXY PROPANOIC ACID METHYL ESTER

Chemical Property:

• Vapor Pressure: 0.00657mmHg at 25°C
• Boiling Point: 271.1°C at 760 mmHg
• Flash Point: 108.3°C
• Density: 1.082g/cm³
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

METHYL 3-PHENOXYPROPIONATE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PHENOXY PROPANOIC ACID METHYL ESTER

There total 14 articles about 3-PHENOXY PROPANOIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

inmethanol + 3-phenoxypropanoic acid (7170-38-9) → methyl 3-phenoxypropanoate (7497-89-4)

Guidance literature:

Reference yield: 92.5%

methanol (67-56-1) + 3-phenoxypropanoic acid (7170-38-9) → methyl 3-phenoxypropanoate (7497-89-4)

Guidance literature:

sulfuric acid; at 140 ℃; for 0.0833333h; Microwave irradiation;

Reference yield: 68.0%

methyl ester (3-hydroxy) propionic acid (6149-41-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → methyl 3-phenoxypropanoate (7497-89-4)

Guidance literature:

With Co(dmgBF₂)₂(CH₃CN)₂; 3-cyano-N-methyl-quinolinium perchlorate; In acetonitrile; at 20 ℃; for 5h; Sealed tube; Inert atmosphere; Irradiation; High pressure;

DOI:10.1021/acs.orglett.7b00463

upstream raw materials:

diazomethane

Phenoxyacetyl chloride

acrylic acid methyl ester

phenol

Downstream raw materials:

3-phenoxypropanoic acid

2-methyl-4-phenoxy-2-butanol

3-phenoxypropanol

acrylic acid methyl ester