N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide

Base Information

• Chemical Name: N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide
• CAS No.: 281197-51-1
• Molecular Formula: C₂₅H₂₈N₆O
• Molecular Weight: 428.537

Synonyms:N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide

Chemical Property of N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide

Chemical Property:

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Technology Process of N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide

There total 2 articles about N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₄-phenyl-1,2(R)-piperazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N4-(1,1-dimethylethyloxycarbonyl)-N2-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide (279237-43-3) + benzaldehyde (100-52-7) → N2-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N4-phenyl-1,2(R)-piperazinecarboxamide (281197-51-1)

Guidance literature:

N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

benzaldehyde; With sodium tris(acetoxy)borohydride; In dichloromethane; acetic acid; at 0 - 20 ℃;

Reference yield:

→ N2-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N4-phenyl-1,2(R)-piperazinecarboxamide (281197-51-1)

Guidance literature:

Reference yield:

N2-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N4-phenyl-1,2(R)-piperazinecarboxamide (281197-51-1) + propionyl chloride (79-03-8) → N-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1-(1-oxopropyl)-4-phenyl(methyl)-2(R)-piperazinedicarboxamide

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 48h;

upstream raw materials:

N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-cyanophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

benzaldehyde

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