pyridin-2-yl sulfurofluoridate

Base Information

• Chemical Name: pyridin-2-yl sulfurofluoridate
• CAS No.: 127827-58-1
• Molecular Formula: C₅H₄FNO₃S
• Molecular Weight: 177.156
• Mol file: 127827-58-1.mol

Synonyms:pyridin-2-yl sulfurofluoridate

Chemical Property of pyridin-2-yl sulfurofluoridate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pyridin-2-yl sulfurofluoridate

There total 3 articles about pyridin-2-yl sulfurofluoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridine (110-86-1) → 2-chloropyridine (109-09-1) + 2-fluoropyridine (372-48-5) + pyridin-2-yl sulfurofluoridate (127827-58-1)

Guidance literature:

With caesium fluoroxysulphate; In chloroform; for 4h; Product distribution; Ambient temperature;

DOI:10.1016/S0040-4039(00)94626-4

Reference yield:

pyridine (110-86-1) → 2-fluoropyridine (372-48-5) + pyridin-2-yl sulfurofluoridate (127827-58-1)

Guidance literature:

With caesium fluoroxysulphate; In cyclohexane; at 22 ℃; for 0.5h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)94626-4

Reference yield:

pyridine (110-86-1) → 2-fluoropyridine (372-48-5) + 2-tert-butoxypyridine (83766-88-5) + pyridin-2-yl sulfurofluoridate (127827-58-1)

Guidance literature:

With caesium fluoroxysulphate; In tert-butyl alcohol; at 50 ℃; for 4h; Product distribution;

DOI:10.1016/S0040-4039(00)94626-4

upstream raw materials:

pyridine

Downstream raw materials:

2-phenylpyridine

2-(4-methylphenyl)pyridine

4-(2-pyridinyl)anisole

4-fluorophenylpyridine