C₄₀H₅₈FN₅O₃

Base Information

Chemical Name:C₄₀H₅₈FN₅O₃
CAS No.:747409-31-0
Molecular Formula:C₄₀H₅₈FN₅O₃
Molecular Weight:675.931
Hs Code.:

C<sub>40</sub>H<sub>58</sub>FN<sub>5</sub>O<sub>3</sub>

Synonyms:C₄₀H₅₈FN₅O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₅₈FN₅O₃

Chemical Property:

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Technology Process of C₄₀H₅₈FN₅O₃

There total 4 articles about C₄₀H₅₈FN₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 674792-27-9
fluoro-(D)-Phe,t-butyl amide dipeptide

: 7693-46-1
4-Nitrophenyl chloroformate

: 747409-31-0
C₄₀H₅₈FN₅O₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 273378-16-8
(1-tert-butoxycarbonyl)-4-cyclohexylpiperidine-4-carboxylic acid

: 747409-31-0
C₄₀H₅₈FN₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / Rh/Al₂O₃ / methanol / 8 h / 70 °C / 3620.13 Torr

1.2: 18.75 h / 0 - 20 °C

2.1: potassium carbonate / methyltertbutyl ether; water / 4 h

2.2: 4 h / 40 - 45 °C

3.1: N-ethylmorpholine;; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 0.17 h

3.2: 2.5 h / 20 °C

4.1: hydrogenchloride / dichloromethane; isopropyl alcohol / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

With N-ethylmorpholine;; hydrogenchloride; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; Rh/Al₂O₃; In methanol; methyltertbutyl ether; dichloromethane; water; isopropyl alcohol; acetonitrile;

Reference yield:

: 674791-75-4
C₇H₈O₃S*C₁₂H₂₁NO₂

: 747409-31-0
C₄₀H₅₈FN₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 2 h / 10 - 17 °C

1.2: 0 - 20 °C / pH 12

2.1: hydrogen / Rh/Al₂O₃ / methanol / 8 h / 70 °C / 3620.13 Torr

2.2: 18.75 h / 0 - 20 °C

3.1: potassium carbonate / methyltertbutyl ether; water / 4 h

3.2: 4 h / 40 - 45 °C

4.1: N-ethylmorpholine;; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 0.17 h

4.2: 2.5 h / 20 °C

5.1: hydrogenchloride / dichloromethane; isopropyl alcohol / 2 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

With N-ethylmorpholine;; hydrogenchloride; sodium hydroxide; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; Rh/Al₂O₃; In tetrahydrofuran; methanol; methyltertbutyl ether; dichloromethane; water; isopropyl alcohol; acetonitrile;