pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Base Information

Chemical Name:pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate
CAS No.:1247847-53-5
Molecular Formula:C₂₁H₁₈Cl₅F₂O₅P
Molecular Weight:596.606
Hs Code.:

Synonyms:pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Suppliers and Price of pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Chemical Property:

Purity/Quality:

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Technology Process of pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

There total 4 articles about pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-86-5,67471-28-7
Pentachlorophenol

: 1247847-54-6
(E)-3-(4-((diethoxyphosphoryl)-difluoromethyl)phenyl)but-2-enoic acid

: 1247847-53-5
pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In ethyl acetate; at 20 ℃; for 24h;

Reference yield:

: 1247847-52-4
tert-butyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

: 1247847-53-5
pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / ethyl acetate / 24 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1021/jm2000882

Reference yield:

: 13329-40-3
4-Iodoacetophenone

: 1247847-53-5
pentachlorophenyl (2E)-3-[4-[(diethoxyphosphinyl)difluoromethyl]phenyl]but-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium tert-butoxide / tetrahydrofuran; hexane; tert-butyl alcohol / 1 h

2.1: cadmium / N,N-dimethyl-formamide / 8 h / Inert atmosphere

2.2: 24 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: dmap; dicyclohexyl-carbodiimide / ethyl acetate / 24 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; cadmium; lithium tert-butoxide; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm2000882