2-cyclohexyl-2,2-diphenylacetaldehyde

Base Information

Chemical Name:2-cyclohexyl-2,2-diphenylacetaldehyde
CAS No.:871878-35-2
Molecular Formula:C₂₀H₂₂O
Molecular Weight:278.394
Hs Code.:

Synonyms:2-cyclohexyl-2,2-diphenylacetaldehyde

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Chemical Property of 2-cyclohexyl-2,2-diphenylacetaldehyde

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Technology Process of 2-cyclohexyl-2,2-diphenylacetaldehyde

There total 7 articles about 2-cyclohexyl-2,2-diphenylacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 94684-49-8
2-cyclohexyl-2,2-diphenylacetonitrile

: 871878-35-2
2-cyclohexyl-2,2-diphenylacetaldehyde

Guidance literature:: With diisobutylaluminium hydride; In cyclohexylamine; toluene; at -78 - 20 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201400969

Reference yield:

: 931-50-0
cyclohexylmagnesium bromide

: 871878-35-2
2-cyclohexyl-2,2-diphenylacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: sulfuric acid

With diethyl ether; sulfuric acid;

Reference yield:

: 626-62-0
Cyclohexyl iodide

: 871878-35-2
2-cyclohexyl-2,2-diphenylacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

1.2: 12 h

2.1: diisobutylaluminium hydride / toluene; cyclohexylamine / 12 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; cyclohexylamine; toluene; mineral oil;
DOI:10.1002/adsc.201400969