4-methoxybenzaldehyde 2-aminoacetylhydrazone

Base Information

Chemical Name:4-methoxybenzaldehyde 2-aminoacetylhydrazone
CAS No.:142071-76-9
Molecular Formula:C₁₀H₁₃N₃O₂
Molecular Weight:207.232
Hs Code.:

Synonyms:4-methoxybenzaldehyde 2-aminoacetylhydrazone

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Chemical Property of 4-methoxybenzaldehyde 2-aminoacetylhydrazone

Chemical Property:

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Technology Process of 4-methoxybenzaldehyde 2-aminoacetylhydrazone

There total 3 articles about 4-methoxybenzaldehyde 2-aminoacetylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 123-11-5
4-methoxy-benzaldehyde

: 14379-80-7
aminoacetic acid hydrazide

: 142071-76-9
4-methoxybenzaldehyde 2-aminoacetylhydrazone

Guidance literature:: In ethanol; for 0.5h;
DOI:10.1007/BF00486809

Reference yield:

: C₁₅H₂₁N₃O₄

: 142071-76-9
4-methoxybenzaldehyde 2-aminoacetylhydrazone

Guidance literature:: With [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2021.116529

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 142071-76-9
4-methoxybenzaldehyde 2-aminoacetylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; sodium acetate / ethanol; water / 20 °C

2: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

With [bis(acetoxy)iodo]benzene; sodium acetate; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2021.116529