Glycerin-monoacetat

Base Information

• Chemical Name: Glycerin-monoacetat
• CAS No.: 93713-40-7
• Molecular Formula: C₅H₁₀O₄
• Molecular Weight: 134.132
• Mol file: 93713-40-7.mol

Synonyms:Glycerin-monoacetat

Chemical Property of Glycerin-monoacetat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Glycerin-monoacetat

There total 38 articles about Glycerin-monoacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

carbon dioxide (124-38-9,18923-20-1) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) + acetonitrile (75-05-8,26809-02-9) → 4-hydroxymethyl-1,3-dioxolan-2-one (931-40-8) + 2-hydroxypropane-1,3-diyl diacetate (105-70-4) + Glycerin-monoacetat (93713-40-7) + 1,2,3-propanetriol 2-acetate (62108-08-1,100-78-7) + diacetin (102-62-5)

Guidance literature:

With La₂O₃ nanocluster on zeolitic imidazolate framework-8; at 150 ℃; for 15h; under 5250.53 Torr; Catalytic behavior; Autoclave;

DOI:10.1039/d0ta12413c

Reference yield:

Benzyl acetate (140-11-4) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → Glycerin-monoacetat (93713-40-7) + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

With sodium hydroxide; at 100 ℃; for 1h;

DOI:10.2174/157017811796504936

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 4-hydroxymethyl-1,3-dioxolan-2-one (931-40-8) + Glycerin-monoacetat (93713-40-7) + 1,2,3-propanetriol 2-acetate (62108-08-1,100-78-7)

Guidance literature:

With La₂Zn₈O₁₁; In acetonitrile; at 170 ℃; for 12h; under 30003 Torr; chemoselective reaction; Mechanism; Autoclave;

DOI:10.1039/c3cy00335c

upstream raw materials:

1,3-diacetoxyacetone

acetyl chloride

glycerol

acetic acid

Downstream raw materials:

Acetanilid

triacetylglycerol

ethyl acetate

glycerol

Refernces

• 1、 Bu, Quan,Cai, Jin,Mao, Hanping,Vasudevan, Srinivasan Vinju. "Ordered mesoporous zirconium silicates as a catalyst for biofuel precursors synthesis". . . Retrieved 2021/11/16.
• 2、 Hou, Zhaoyin,Jiang, Yuanyuan,Long, Yihua,Wang, Zhengbao,Ye, Boyong,Zhao, Huaiyuan,Zhou, Ruru. "A highly active and stable organic-inorganic combined solid acid for the transesterification of glycerol under mild conditions". . p. 1772 - 1781. Retrieved 2021/06/28.