5 -chloro-N'-phenyl valeryl hydrazide

Base Information

• Chemical Name: 5 -chloro-N'-phenyl valeryl hydrazide
• CAS No.: 91244-46-1
• Molecular Formula: C₁₁H₁₅ClN₂O
• Molecular Weight: 226.706
• Mol file: 91244-46-1.mol

Synonyms:5 -chloro-N'-phenyl valeryl hydrazide

Chemical Property of 5 -chloro-N'-phenyl valeryl hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5 -chloro-N'-phenyl valeryl hydrazide

There total 1 articles about 5 -chloro-N'-phenyl valeryl hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

5-Chlorovaleroyl chloride (1575-61-7) + phenylhydrazine (100-63-0) → 5 -chloro-N'-phenyl valeryl hydrazide (91244-46-1)

Guidance literature:

With sodium carbonate; In dichloromethane; water; at 0 - 20 ℃;

Reference yield: 77.0%

dimethyl acetylenedicarboxylate (762-42-5) + 5 -chloro-N'-phenyl valeryl hydrazide (91244-46-1) → dimethyl 5-(4-chlorobutyl)-1-phenyl-1H-pyrazole-3,4-dicarboxylate (1616351-65-5)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium acetate; In acetonitrile; at 60 ℃; for 5h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/ol501402p

Reference yield: 76.0%

hydrogen ethyl malonate (1071-46-1) + 5 -chloro-N'-phenyl valeryl hydrazide (91244-46-1) → ethyl 3-(2-(5-chloropentanoyl)-1-phenylhydrazinyl)-3-oxopropanoate

Guidance literature:

With thionyl chloride; In dichloromethane; at 20 ℃;

upstream raw materials:

5-Chlorovaleroyl chloride

phenylhydrazine

Downstream raw materials:

dimethyl 5-(4-chlorobutyl)-1-phenyl-1H-pyrazole-3,4-dicarboxylate