3-phenyl-3-<4-phenoxy>propanoic acid

Base Information

Chemical Name:3-phenyl-3-<4-phenoxy>propanoic acid
CAS No.:127086-75-3
Molecular Formula:C₂₀H₂₂O₅
Molecular Weight:342.392
Hs Code.:

3-phenyl-3-<4-<isopropoxycarbonyl)methyl>phenoxy>propanoic acid

Synonyms:3-phenyl-3-<4-phenoxy>propanoic acid

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Chemical Property of 3-phenyl-3-<4-phenoxy>propanoic acid

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Technology Process of 3-phenyl-3-<4-phenoxy>propanoic acid

There total 6 articles about 3-phenyl-3-<4-phenoxy>propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

: tert-butyl 3-phenyl-3-<4-phenoxy>propanoate

: 127086-75-3
3-phenyl-3-<4-phenoxy>propanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ja00175a039

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 127086-75-3
3-phenyl-3-<4-phenoxy>propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / conc. H₂SO₄ / Heating

2: 1.) KH, 2.) 18-crown-6 / 1.) THF, RT, 20 min, 2.) RT

3: 98 percent / H₂, / 10percent Pd/C / ethyl acetate / 3 h

4: 99.8 percent / trifluoroacetic acid / CH₂Cl₂ / 3 h / 0 °C

With 18-crown-6 ether; sulfuric acid; hydrogen; potassium hydride; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ja00175a039

Reference yield:

: 41997-33-5
iso-propyl 4-hydroxyphenylacetate

: 127086-75-3
3-phenyl-3-<4-phenoxy>propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH, 2.) 18-crown-6 / 1.) THF, RT, 20 min, 2.) RT

2: 98 percent / H₂, / 10percent Pd/C / ethyl acetate / 3 h

3: 99.8 percent / trifluoroacetic acid / CH₂Cl₂ / 3 h / 0 °C

With 18-crown-6 ether; hydrogen; potassium hydride; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ja00175a039