methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

Base Information

Chemical Name:methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate
CAS No.:1596341-57-9
Molecular Formula:C₂₂H₂₉F₃O₄
Molecular Weight:414.465
Hs Code.:

Synonyms:methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

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Chemical Property of methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

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Technology Process of methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

There total 11 articles about methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1596341-56-8
methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

: 1596341-57-9
methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethyl acetate; for 48h;

Reference yield:

: 1403382-22-8
ethyl 2-{3-fluoro-2-[(trifluoromethane) sulfonyloxy]-6-(trifluoromethyl)phenyl)-2-oxoacetate

: 1596341-57-9
methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 2 h / 65 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 60 °C / Inert atmosphere

3: N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

4: sodium tetrahydroborate / diethylene glycol dimethyl ether / 1 h / 0 °C

5: perchloric acid / water / 1 h / 0 °C

6: hydrogen; palladium on activated charcoal / ethyl acetate / 48 h

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; perchloric acid; palladium on activated charcoal; hydrogen; sodium hydride; potassium carbonate; In tetrahydrofuran; diethylene glycol dimethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1596341-54-6
ethyl 2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-fluoro-6-(trifluoromethyl)phenyl]-2-oxoacetate

: 1596341-57-9
methyl 2-(tert-butoxy)-2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-hydroxy-6-(trifluoromethyl)phenyl]acetate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 60 °C / Inert atmosphere

2: N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

3: sodium tetrahydroborate / diethylene glycol dimethyl ether / 1 h / 0 °C

4: perchloric acid / water / 1 h / 0 °C

5: hydrogen; palladium on activated charcoal / ethyl acetate / 48 h

With sodium tetrahydroborate; perchloric acid; palladium on activated charcoal; hydrogen; sodium hydride; In diethylene glycol dimethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;