methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

Base Information

Chemical Name:methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate
CAS No.:1596341-56-8
Molecular Formula:C₂₉H₃₅F₃O₄
Molecular Weight:504.59
Hs Code.:

Synonyms:methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

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Chemical Property of methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

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Technology Process of methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

There total 11 articles about methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 540-88-5
acetic acid tert-butyl ester

: 1596341-55-7
methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-hydroxyacetate

: 1596341-56-8
methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

Guidance literature:: With perchloric acid; In water; at 0 ℃; for 1h;

Reference yield:

: 1403382-22-8
ethyl 2-{3-fluoro-2-[(trifluoromethane) sulfonyloxy]-6-(trifluoromethyl)phenyl)-2-oxoacetate

: 1596341-56-8
methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 2 h / 65 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 60 °C / Inert atmosphere

3: N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

4: sodium tetrahydroborate / diethylene glycol dimethyl ether / 1 h / 0 °C

5: perchloric acid / water / 1 h / 0 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; perchloric acid; sodium hydride; potassium carbonate; In tetrahydrofuran; diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1596341-54-6
ethyl 2-[2-(4,4-dimethylcyclohex-1-en-1-yl)-3-fluoro-6-(trifluoromethyl)phenyl]-2-oxoacetate

: 1596341-56-8
methyl 2-[3-(benzyloxy)-2-(4,4-dimethylcyclohex-1-en-1-yl)-6-(trifluoromethyl)phenyl]-2-(tert-butoxy)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 60 °C / Inert atmosphere

2: N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

3: sodium tetrahydroborate / diethylene glycol dimethyl ether / 1 h / 0 °C

4: perchloric acid / water / 1 h / 0 °C

With sodium tetrahydroborate; perchloric acid; sodium hydride; In diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide; mineral oil;