methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

Base Information

Chemical Name:methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate
CAS No.:1411983-21-5
Molecular Formula:C₁₇H₂₁N₃O₆
Molecular Weight:363.37
Hs Code.:

Synonyms:methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

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Chemical Property of methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

Chemical Property:

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Technology Process of methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

There total 2 articles about methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 616-45-5
2-pyrrolidinon

: 1411983-22-6
methyl 3-bromo-6-(2,2-dimethylpropionylamino)-2-nitro-benzoate

: 1411983-21-5
methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

Guidance literature:: With potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide; In toluene; at 110 ℃; for 5h; Cooling with ice;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 1411983-21-5
methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 3 h / 20 °C

2: potassium carbonate; N,N`-dimethylethylenediamine / copper(l) iodide / toluene / 5 h / 110 °C / Cooling with ice

With pyridine; potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide; In dichloromethane; toluene;

Reference yield:

: 1411983-21-5
methyl 6-(2,2-dimethylpropionylamino)-2-nitro-3-(2-oxopyrrolidin-1-yl)benzoate

: 1411982-80-3
methyl 6-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-2,3-dihydro-1H-benzo[d]pyrrolo[1,2-a]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; iron / 2.5 h / 115 °C

2: sulfuric acid / methanol / 44 h / Reflux

3: pyridine / dichloromethane / 24 h / 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; di-tert-butylneopentylphosphonium tetrafluoroborate / 1,4-dioxane; dimethyl sulfoxide / 2 h / 95 °C / Inert atmosphere

With pyridine; sulfuric acid; iron; acetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; di-tert-butylneopentylphosphonium tetrafluoroborate; In 1,4-dioxane; methanol; dichloromethane; dimethyl sulfoxide;