(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

Base Information

Chemical Name:(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester
CAS No.:1610691-86-5
Molecular Formula:C₁₇H₂₆N₂O₆
Molecular Weight:354.403
Hs Code.:

Synonyms:(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

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Chemical Property of (R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

Chemical Property:

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Technology Process of (R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

There total 4 articles about (R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1610691-82-1
(R)-N-(2-chloroacetyl)-4-methoxyphenylalanine methyl ester

: 22483-09-6
2,2-dimethoxyethylamine

: 1610691-86-5
(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

Guidance literature:: With sodium iodide; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2014.04.045

Reference yield:

: 68856-96-2
N-(tert-butoxycarbonyl)-O-methyl-D-tyrosine

: 1610691-86-5
(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2: hydrogenchloride / ethyl acetate / 3 h / 20 °C

3: triethylamine / dichloromethane / 1 h / 0 - 20 °C

4: sodium iodide / dichloromethane / 48 h / 20 °C

With hydrogenchloride; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.04.045

Reference yield:

: 94790-24-6
(2R)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)propionic acid methyl ester

: 1610691-86-5
(R)-N-[N-(2,2-dimethoxyethyl)glycinyl]-4-methoxyphenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 0 - 20 °C

3: sodium iodide / dichloromethane / 48 h / 20 °C

With hydrogenchloride; triethylamine; sodium iodide; In dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2014.04.045