C₃₇H₄₂Cl₃NO₁₉

Base Information

Chemical Name:C₃₇H₄₂Cl₃NO₁₉
CAS No.:1426099-71-9
Molecular Formula:C₃₇H₄₂Cl₃NO₁₉
Molecular Weight:911.095
Hs Code.:

C<sub>37</sub>H<sub>42</sub>Cl<sub>3</sub>NO<sub>19</sub>

Synonyms:C₃₇H₄₂Cl₃NO₁₉

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Chemical Property of C₃₇H₄₂Cl₃NO₁₉

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Technology Process of C₃₇H₄₂Cl₃NO₁₉

There total 12 articles about C₃₇H₄₂Cl₃NO₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1138124-35-2
C₄₄H₄₈Cl₃NO₁₉

: 1426099-71-9
C₃₇H₄₂Cl₃NO₁₉

Guidance literature:: With palladium 10% on activated carbon; hydrogen; trichloroacetic acid; In methanol; for 0.25h;
DOI:10.1021/ja4000933

Reference yield:

: 176299-96-0
4-methoxyphenyl 4,6-O-benzylidene-β-D-galactopyranoside

: 1426099-71-9
C₃₇H₄₂Cl₃NO₁₉

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 2 h / -40 °C / Inert atmosphere

2: 2,6-di-tert-butyl-pyridine; 1,2-dimethoxy-4-(2-propenyl)benzene; trifluoromethylsulfonic anhydride / dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Molecular sieve

3: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -78 °C / Molecular sieve; Inert atmosphere

4: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: hydrogen; palladium 10% on activated carbon; trichloroacetic acid / methanol / 0.25 h

With pyridine; triethylsilane; dmap; 2,6-di-tert-butyl-pyridine; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; 1,2-dimethoxy-4-(2-propenyl)benzene; palladium 10% on activated carbon; hydrogen; trichloroacetic acid; In methanol; dichloromethane;
DOI:10.1021/ja4000933

Reference yield:

: 1426099-68-4
C₂₇H₂₆O₉

: 1426099-71-9
C₃₇H₄₂Cl₃NO₁₉

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-di-tert-butyl-pyridine; 1,2-dimethoxy-4-(2-propenyl)benzene; trifluoromethylsulfonic anhydride / dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Molecular sieve

2: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -78 °C / Molecular sieve; Inert atmosphere

3: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: hydrogen; palladium 10% on activated carbon; trichloroacetic acid / methanol / 0.25 h

With pyridine; triethylsilane; dmap; 2,6-di-tert-butyl-pyridine; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; 1,2-dimethoxy-4-(2-propenyl)benzene; palladium 10% on activated carbon; hydrogen; trichloroacetic acid; In methanol; dichloromethane;
DOI:10.1021/ja4000933