O,O-diethyl Se-ethyl selenophosphate

Base Information

• Chemical Name: O,O-diethyl Se-ethyl selenophosphate
• CAS No.: 39181-35-6
• Molecular Formula: C₆H₁₅O₃PSe
• Molecular Weight: 245.117

Synonyms:O,O-diethyl Se-ethyl selenophosphate

Chemical Property of O,O-diethyl Se-ethyl selenophosphate

Chemical Property:

Purity/Quality:

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Technology Process of O,O-diethyl Se-ethyl selenophosphate

There total 2 articles about O,O-diethyl Se-ethyl selenophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

O,O-diethyl phosphoroselenoic acid (7452-28-0) → O,O,O-triethylselenophosphate (2651-89-0) + O,O-diethyl Se-ethyl selenophosphate (39181-35-6) + tetra-O-ethyl asym-monoselenopyrophosphate (26905-48-6) + N,N'-dicyclohexylselenourea (34656-93-4)

Guidance literature:

With dicyclohexyl-carbodiimide; In diethyl ether; for 48h; Ambient temperature;

DOI:10.1021/jo00179a028

Reference yield: 90.0%

O,O-diethyl phosphoroselenoic acid (7452-28-0) + dicyclohexyl-carbodiimide (538-75-0) → O,O,O-triethylselenophosphate (2651-89-0) + O,O-diethyl Se-ethyl selenophosphate (39181-35-6) + tetra-O-ethyl asym-monoselenopyrophosphate (26905-48-6) + N,N'-dicyclohexylselenourea (34656-93-4)

Guidance literature:

In diethyl ether; for 48h; Mechanism; Product distribution; Ambient temperature; other solvents;

DOI:10.1021/jo00179a028

Reference yield:

O,O-diethyl Se-ethyl selenophosphate (39181-35-6) + ethanol (64-17-5) → triethyl phosphate (78-40-0)

Guidance literature:

With mercury(II) trifluoroacetate; In acetonitrile; for 0.166667h; Ambient temperature;

DOI:10.1021/jo00048a050

upstream raw materials:

O,O-diethyl phosphoroselenoic acid

dicyclohexyl-carbodiimide

Downstream raw materials:

triethyl phosphate

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