{4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane

Base Information

• Chemical Name: {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane
• CAS No.: 1032476-06-4
• Molecular Formula: C₂₀H₃₆OSi₂
• Molecular Weight: 348.676

Synonyms:{4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane

Chemical Property of {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane

There total 1 articles about {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chloro-trimethyl-silane (75-77-4) + 2-allyl-3-methyl-2-cyclohexen-1-one (17605-08-2) + 4-bromo-1-trimethylsilylbut-1-yne (69361-41-7) → {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane (1032476-06-4)

Guidance literature:

4-bromo-1-trimethylsilylbut-1-yne; With magnesium; ethylene dibromide; In tetrahydrofuran; for 1h; Heating;

With copper(l) iodide; In tetrahydrofuran; at -78 ℃; for 0.5h;

chloro-trimethyl-silane; 2-allyl-3-methyl-2-cyclohexen-1-one; With triethylamine; In tetrahydrofuran; at -78 - 20 ℃; for 12h;

DOI:10.1002/ejoc.200700986

Reference yield: 78.0%

{4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane (1032476-06-4) → 2-bromo-2-allyl-3-methyl-3-(4-trimethylsilyl-3-butynyl)-1-cyclohexanone (1032476-07-5)

Guidance literature:

With iron(III) chloride; sodium bromide; In acetonitrile; at 0 - 20 ℃; for 4h;

DOI:10.1002/ejoc.200700986

Reference yield: 60.0%

{4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane (1032476-06-4) → 2-iodo-2-allyl-3-methyl-3-(4-trimethylsilyl-3-butynyl)-1-cyclohexanone

Guidance literature:

With iron(III) chloride; sodium iodide; In acetonitrile; at 0 - 20 ℃;

DOI:10.1016/j.tet.2006.01.067

upstream raw materials:

chloro-trimethyl-silane

2-allyl-3-methyl-2-cyclohexen-1-one

4-bromo-1-trimethylsilylbut-1-yne

Downstream raw materials:

2-bromo-2-allyl-3-methyl-3-(4-trimethylsilyl-3-butynyl)-1-cyclohexanone

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1032476-06-4 {4-[2-allyl-1-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl]but-1-ynyl}trimethylsilane

Send

Send

Metric Ton KG G Pound L ML

Send

Send