1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

Base Information

Chemical Name:1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form
CAS No.:87878-21-5
Molecular Formula:C₂₂H₁₆ClN₇O₂
Molecular Weight:445.868
Hs Code.:

Synonyms:1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

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Chemical Property of 1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

There total 4 articles about 1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 85093-49-8
2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

: 87878-21-5
1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

Guidance literature:: With potassium hydroxide; dihydrogen peroxide; In 1,4-dioxane; water; for 1h;

Reference yield: 30.0%

: 85093-49-8
2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

: 55134-99-1
2-(4-nitrophenyl)-5-phenyl-2H-tetrazole

: 40227-54-1
4-chloro-2-methylphthalazin-1-(2H)-one

: 87878-21-5
1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

Guidance literature:: With nitric acid; for 0.166667h;

Reference yield:

: 25939-13-3
N-(p-nitrophenyl)benzohydrazonoyl chloride

: 87878-21-5
1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine / benzene / 4 h

2: 80 percent / 2N KOH, 30percent H₂O₂ / H₂O; dioxane / 1 h

With potassium hydroxide; dihydrogen peroxide; triethylamine; In 1,4-dioxane; water; benzene;