2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

Base Information

• Chemical Name: 2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine
• CAS No.: 85093-49-8
• Molecular Formula: C₂₂H₁₈ClN₇O₂
• Molecular Weight: 447.884
• Mol file: 85093-49-8.mol

Synonyms:2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

Chemical Property of 2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine

There total 1 articles about 2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-(p-nitrophenyl)benzohydrazonoyl chloride (25939-13-3) + 2-methyl-4-chloro-1-phthalazinone hydrazone (64640-64-8) → (2-methyl-4-chloro-1,2-dihydrophthalazine)-1-spiro-5'-<1-(4'-nitrophenyl)-4'-amino-1',5'-dihydro-1',2',4'-triazole> (85093-50-1) + 2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine (85093-49-8)

Guidance literature:

With triethylamine; In benzene; for 4h;

Reference yield: 80.0%

2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine (85093-49-8) → 1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form (87878-21-5)

Guidance literature:

With potassium hydroxide; dihydrogen peroxide; In 1,4-dioxane; water; for 1h;

Reference yield: 30.0%

2-(4-nitrophenyl)-4-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)benzohydrazidine (85093-49-8) → 2-(4-nitrophenyl)-5-phenyl-2H-tetrazole (55134-99-1) + 4-chloro-2-methylphthalazin-1-(2H)-one (40227-54-1) + 1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form (87878-21-5)

Guidance literature:

With nitric acid; for 0.166667h;

upstream raw materials:

N-(p-nitrophenyl)benzohydrazonoyl chloride

2-methyl-4-chloro-1-phthalazinone hydrazone

Downstream raw materials:

2-(4-nitrophenyl)-5-phenyl-2H-tetrazole

4-chloro-2-methylphthalazin-1-(2H)-one

1-(4-nitrophenyl)-3-phenyl-5-(2-methyl-4-chloro-1,2-dihydro-1-phthalazinylidene)-3-phenylformazan EE'E'' form