4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

Base Information

Chemical Name:4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester
CAS No.:166764-44-9
Molecular Formula:C₁₅H₂₀ClNO₅Si
Molecular Weight:357.866
Hs Code.:

Synonyms:4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

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Chemical Property of 4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

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Technology Process of 4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

There total 3 articles about 4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 75-77-4
chloro-trimethyl-silane

: 155719-53-2
4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid

: 166764-44-9
4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃;

Reference yield:

: 108-90-7
chlorobenzene

: 166764-44-9
4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 1,2-dichloro-ethane / 4 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With triethylamine; In dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 79686-90-1
N-(methoxycarbonyl)aspartic anhydride

: 166764-44-9
4-(4-chlorophenyl)-2-methoxycarbonylamino-4-oxobutanoic acid trimethylsilyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 1,2-dichloro-ethane / 4 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With triethylamine; In dichloromethane; 1,2-dichloro-ethane;