C₂₈H₂₈ClN₇O₄S

Base Information

Chemical Name:C₂₈H₂₈ClN₇O₄S
CAS No.:1365992-82-0
Molecular Formula:C₂₈H₂₈ClN₇O₄S
Molecular Weight:594.094
Hs Code.:

C<sub>28</sub>H<sub>28</sub>ClN<sub>7</sub>O<sub>4</sub>S

Synonyms:C₂₈H₂₈ClN₇O₄S

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Chemical Property of C₂₈H₂₈ClN₇O₄S

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Technology Process of C₂₈H₂₈ClN₇O₄S

There total 14 articles about C₂₈H₂₈ClN₇O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1365992-73-9
3-chloro-2-(4-chlorothiazolo[5,4-c]pyridine-2-yl)-benzonitrile

: 1364663-30-8
(6-amino-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butyl ester

: 1365992-82-0
C₂₈H₂₈ClN₇O₄S

Guidance literature:: With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 80 ℃; for 16h; Inert atmosphere;

Reference yield:

: 17282-04-1
2-chloro-3-fluoropyridine

: 1365992-82-0
C₂₈H₂₈ClN₇O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 4.67 h / -70 °C

1.2: 2 h / -70 - 20 °C

2.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1.5 h / Inert atmosphere; Reflux

3.1: thionyl chloride / 18 h / 100 °C / Inert atmosphere

4.1: thiourea; pyridine / isopropyl alcohol / 3 h / Inert atmosphere; Reflux

4.2: 1.5 h / Reflux

5.1: 1-methyl-pyrrolidin-2-one / 0.33 h / 150 °C

6.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

With pyridine; thionyl chloride; caesium carbonate; thiourea; lithium diisopropyl amide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; n-heptane; ethylbenzene; isopropyl alcohol;

Reference yield:

: 148639-07-0
2-chloro-3-fluoro-4-iodopyridyne

: 1365992-82-0
C₂₈H₂₈ClN₇O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1.5 h / Inert atmosphere; Reflux

2.1: thionyl chloride / 18 h / 100 °C / Inert atmosphere

3.1: thiourea; pyridine / isopropyl alcohol / 3 h / Inert atmosphere; Reflux

3.2: 1.5 h / Reflux

4.1: 1-methyl-pyrrolidin-2-one / 0.33 h / 150 °C

5.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

With pyridine; thionyl chloride; caesium carbonate; thiourea; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; isopropyl alcohol;