trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

Base Information

Chemical Name:trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde
CAS No.:96184-79-1
Molecular Formula:C₁₆H₁₉NO
Molecular Weight:241.333
Hs Code.:

Synonyms:trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

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Chemical Property of trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

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Technology Process of trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

There total 9 articles about trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96184-81-5
(+/-)-cyclohexanone-4-carboxaldehyde

: 96184-79-1
trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 33 g / 1,2-dimethoxy-ethane / 3.5 h / Ambient temperature

2: 22.6 g / hydrogen / 5percent palladium-on-carbon / ethanol; toluene

3: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

4: 2N HCl / tetrahydrofuran / 0.5 h / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; toluene;

Reference yield:

: p-[2-(trans-4-hydroxymethylcyclohexyl)ethyl]benzonitrile

: 79-37-8
oxalyl dichloride

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 96184-79-1
trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

Guidance literature:: With triethylamine; In dichloromethane; water;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 96184-79-1
trans-4-[2-(p-cyanophenyl)ethyl]cyclohexanecarboxaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / tetrahydrofuran; various solvent(s) / 2 h / Ambient temperature

2: 85 percent / acetic acid; H₂O / 1 h / Heating

3: 33 g / 1,2-dimethoxy-ethane / 3.5 h / Ambient temperature

4: 22.6 g / hydrogen / 5percent palladium-on-carbon / ethanol; toluene

5: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

6: 2N HCl / tetrahydrofuran / 0.5 h / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; acetic acid; toluene;