((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Base Information

Chemical Name:((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate
CAS No.:1563184-71-3
Molecular Formula:C₁₆H₂₅N₃O₁₂S₃
Molecular Weight:547.585
Hs Code.:

Synonyms:((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Suppliers and Price of ((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

There total 6 articles about ((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1563184-60-0
5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

: 141-43-5
ethanolamine

: 1563184-71-3
((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid; With oxalyl dichloride; magnesium oxide; N,N-dimethyl-formamide; In dichloromethane; acetonitrile; at 0 - 20 ℃; for 4h;

ethanolamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 0.333333h;

Reference yield:

: 34036-07-2
3,4 difluorobenzaldehyde

: 1563184-71-3
((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: Multi-step reaction with 8 steps

1.1: dimethyl sulfoxide / 3 h / 75 °C / Inert atmosphere

2.1: sodium dihydrogen phosphate monohydrate; dihydrogen peroxide; sodium chlorite; hydrogenchloride / acetonitrile; water / 0 - 20 °C

3.1: sulfuric acid; nitric acid / 4 h / 45 °C

4.1: perchloric acid / acetonitrile / 48 h / 20 °C

5.1: dimethyl sulfoxide / 2 h / 20 °C

6.1: triethylamine / dichloromethane / 0.33 h / 0 °C

7.1: trifluoroacetic acid / dichloromethane / 5 - 20 °C

8.1: N,N-dimethyl-formamide; magnesium oxide; oxalyl dichloride / dichloromethane; acetonitrile / 4 h / 0 - 20 °C

8.2: 0.33 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; perchloric acid; sodium dihydrogen phosphate monohydrate; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; nitric acid; magnesium oxide; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 185945-88-4
3-fluoro-4-(methylsulfonyl)benzoic acid

: 1563184-71-3
((5-((2-hydroxyethyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid; nitric acid / 4 h / 45 °C

2.1: perchloric acid / acetonitrile / 48 h / 20 °C

3.1: dimethyl sulfoxide / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 0.33 h / 0 °C

5.1: trifluoroacetic acid / dichloromethane / 5 - 20 °C

6.1: N,N-dimethyl-formamide; magnesium oxide; oxalyl dichloride / dichloromethane; acetonitrile / 4 h / 0 - 20 °C

6.2: 0.33 h / 0 - 20 °C

With perchloric acid; oxalyl dichloride; sulfuric acid; nitric acid; magnesium oxide; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; acetonitrile;