5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

Base Information

Chemical Name:5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid
CAS No.:1563184-60-0
Molecular Formula:C₁₄H₂₀N₂O₁₂S₃
Molecular Weight:504.517
Hs Code.:

Synonyms:5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

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Chemical Property of 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

Chemical Property:

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Technology Process of 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

There total 6 articles about 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1563184-59-7
tert-butyl 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

: 1563184-60-0
5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 5 - 20 ℃;

Reference yield:

: 34036-07-2
3,4 difluorobenzaldehyde

: 1563184-60-0
5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: dimethyl sulfoxide / 3 h / 75 °C / Inert atmosphere

2: sodium dihydrogen phosphate monohydrate; dihydrogen peroxide; sodium chlorite; hydrogenchloride / acetonitrile; water / 0 - 20 °C

3: sulfuric acid; nitric acid / 4 h / 45 °C

4: perchloric acid / acetonitrile / 48 h / 20 °C

5: dimethyl sulfoxide / 2 h / 20 °C

6: triethylamine / dichloromethane / 0.33 h / 0 °C

7: trifluoroacetic acid / dichloromethane / 5 - 20 °C

With hydrogenchloride; sodium chlorite; perchloric acid; sodium dihydrogen phosphate monohydrate; sulfuric acid; dihydrogen peroxide; nitric acid; triethylamine; trifluoroacetic acid; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 185945-88-4
3-fluoro-4-(methylsulfonyl)benzoic acid

: 1563184-60-0
5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid / 4 h / 45 °C

2: perchloric acid / acetonitrile / 48 h / 20 °C

3: dimethyl sulfoxide / 2 h / 20 °C

4: triethylamine / dichloromethane / 0.33 h / 0 °C

5: trifluoroacetic acid / dichloromethane / 5 - 20 °C

With perchloric acid; sulfuric acid; nitric acid; triethylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; acetonitrile;