tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

Base Information

Chemical Name:tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate
CAS No.:1563184-57-5
Molecular Formula:C₁₆H₂₄N₂O₈S
Molecular Weight:404.441
Hs Code.:

Synonyms:tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

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Chemical Property of tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

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Technology Process of tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

There total 9 articles about tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1563184-56-4
tert-butyl 5-fluoro-4-(methylsulfonyl)-2-nitrobenzoate

: 111-42-2
2,2'-iminobis[ethanol]

: 1563184-57-5
tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 2h;

Reference yield:

: 1563184-56-4
tert-butyl 5-fluoro-4-(methylsulfonyl)-2-nitrobenzoate

: 111-42-2
2,2'-iminobis[ethanol]

: 1563184-57-5
tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

: 1563184-58-6
tert-butyl 5-(2-((2-hydroxyethyl)amino)ethoxy)-4-(methylsulfonyl)-2-nitrobenzoate

Guidance literature:: In dimethyl sulfoxide; at 40 - 50 ℃;

Reference yield:

: 34036-07-2
3,4 difluorobenzaldehyde

: 1563184-57-5
tert-butyl 5-(bis(2-hydroxyethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / 3 h / 75 °C / Inert atmosphere

2: sodium dihydrogen phosphate monohydrate; dihydrogen peroxide; sodium chlorite; hydrogenchloride / acetonitrile; water / 0 - 20 °C

3: sulfuric acid; nitric acid / 4 h / 45 °C

4: perchloric acid / acetonitrile / 48 h / 20 °C

5: dimethyl sulfoxide / 2 h / 20 °C

With hydrogenchloride; sodium chlorite; perchloric acid; sodium dihydrogen phosphate monohydrate; sulfuric acid; dihydrogen peroxide; nitric acid; In water; dimethyl sulfoxide; acetonitrile;