C₁₅H₁₈ClFO₃

Base Information

Chemical Name:C₁₅H₁₈ClFO₃
CAS No.:1541198-14-4
Molecular Formula:C₁₅H₁₈ClFO₃
Molecular Weight:300.758
Hs Code.:

C<sub>15</sub>H<sub>18</sub>ClFO<sub>3</sub>

Synonyms:C₁₅H₁₈ClFO₃

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Chemical Property of C₁₅H₁₈ClFO₃

Chemical Property:

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Technology Process of C₁₅H₁₈ClFO₃

There total 5 articles about C₁₅H₁₈ClFO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541198-05-3
(4-(3-chloro-5-(1,3-dioxolan-2-yl)phenyl)tetrahydro-2H-pyran-4-yl)methanol

: 1541198-14-4
C₁₅H₁₈ClFO₃

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -60 ℃; for 1h; Inert atmosphere;

Reference yield:

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 1541198-14-4
C₁₅H₁₈ClFO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

3.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.08 h / 0 - 25 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 25 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -60 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; hexane; dichloromethane; di-isopropyl ether; toluene;

Reference yield:

: 188813-05-0
3-bromo-5-chloro-benzaldehyde

: 1541198-14-4
C₁₅H₁₈ClFO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

2.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.08 h / 0 - 25 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 25 °C

4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -60 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; hexane; dichloromethane; toluene;