4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine

Base Information

• Chemical Name: 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine
• CAS No.: 1168207-56-4
• Molecular Formula: C₁₆H₂₄ClNO₂Si
• Molecular Weight: 325.911

Synonyms:4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine

Chemical Property of 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine

Chemical Property:

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Technology Process of 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine

There total 3 articles about 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

chloro-trimethyl-silane (75-77-4) + (4-(4-chlorophenyl)-6,6-dimethyl-5,6-dihydro-4H-1,2-oxazin-3-yl)methanol (1168207-69-9) → 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine (1168207-56-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.03.082

Reference yield:

C16H24ClNO2Si (1168207-46-2) → 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine (1168207-56-4)

Guidance literature:

With water; In chloroform; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2009.03.082

Reference yield:

C16H24ClNO2Si (1168207-46-2) → 4-(4-chlorophenyl)-6,6-dimethyl-3-((trimethylsilyloxy)methyl)-5,6-dihydro-4H-1,2-oxazine (1168207-56-4) + 4-(4-chlorophenyl)-6,6-dimethyl-dihydro-2H-pyran-3(4H)-one O-trimethylsilyl oxime (1168207-75-7)

Guidance literature:

With water; In chloroform; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2009.03.082

upstream raw materials:

C₁₆H₂₄ClNO₂Si

chloro-trimethyl-silane

(4-(4-chlorophenyl)-6,6-dimethyl-5,6-dihydro-4H-1,2-oxazin-3-yl)methanol

Downstream raw materials:

(4-(4-chlorophenyl)-6,6-dimethyl-5,6-dihydro-4H-1,2-oxazin-3-yl)methanol

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