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Technology Process of {((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)

{((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)

Base Information
  • Chemical Name:{((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)
  • CAS No.:109786-99-4
  • Molecular Formula:C2H3O2*C72H93CoN9O
  • Molecular Weight:1218.63
  • Hs Code.:
{((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>4</sub>N<sub>4</sub>)Co(NH<sub>3</sub>)((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>6</sub>N<sub>3</sub>NO)}<sup>(1+)</sup>*CH<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>={((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>4</sub>N<sub>4</sub>)Co(NH<sub>3</sub>)((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>6</sub>N<sub>3</sub>NO)}(CH<sub>3</sub>CO<sub>2</sub>)

Synonyms:{((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)

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Chemical Property of {((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)
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Technology Process of {((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)

There total 1 articles about {((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2,3,7,8,12,13,17,18-octaethyl-21H,23H-porphine cobalt(II)
17632-19-8

2,3,7,8,12,13,17,18-octaethyl-21H,23H-porphine cobalt(II)

octaethylporphyrin N-oxide
67514-01-6

octaethylporphyrin N-oxide

dichloromethane
75-09-2

dichloromethane

ammonia
7664-41-7

ammonia

sodium acetate
127-09-3

sodium acetate

{((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>4</sub>N<sub>4</sub>)Co(NH<sub>3</sub>)((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>6</sub>N<sub>3</sub>NO)}<sup>(1+)</sup>*CH<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>={((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>4</sub>N<sub>4</sub>)Co(NH<sub>3</sub>)((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>6</sub>N<sub>3</sub>NO)}(CH<sub>3</sub>CO<sub>2</sub>)
109786-99-4

{((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(1+)*CH3CO2(1-)={((C2H5)8C20H4N4)Co(NH3)((C2H5)8C20H6N3NO)}(CH3CO2)

Guidance literature:
In methanol; dichloromethane; addn. of a methanol soln. (2ml) sucessively satd. with NH3 and Na-acetate to a soln. of 0.03 Co(II) octaetylporphyrin , addn. of 0.04mmol octaethylporphyrin-N-oxide, stirring 1h under Ar, removal of solvent in vac.;; dissolving in 50ml CH2Cl2, washing with H2O, drying over Na2SO4, filtration, concn., chromatography on a SiO2-column, eluation of product with CH2Cl2/5% methanol, removal of solvent in vac., recrystn. from CH2Cl2/n-hexane;;
upstream raw materials:

2,3,7,8,12,13,17,18-octaethyl-21H,23H-porphine cobalt(II)

octaethylporphyrin N-oxide

dichloromethane

ammonia

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