2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

Base Information

Chemical Name:2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol
CAS No.:121056-89-1
Molecular Formula:C₂₆H₅₃NO₄Si₃
Molecular Weight:527.968
Hs Code.:

Synonyms:2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

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Chemical Property of 2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

Chemical Property:

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Technology Process of 2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

There total 6 articles about 2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121056-90-4
Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

: 121056-89-1
2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1021/ja00198a040

Reference yield:

: 99-24-1
methyl galloate

: 121056-89-1
2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / imidazole / dimethylformamide / 20 h

2: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

4: ZnI₂ / 4 h / Ambient temperature

5: LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; pyridinium chlorochromate; zinc(II) iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00198a040

Reference yield:

: 121056-97-1
methyl 3,4,5-tris<(tert-butyldimethylsilyl)oxy>benzoate

: 121056-89-1
2-Amino-1-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

2: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

3: ZnI₂ / 4 h / Ambient temperature

4: LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

With lithium aluminium tetrahydride; pyridinium chlorochromate; zinc(II) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00198a040