N-(ethyldiphenylgermylmethyl)benzylamine

Base Information

Chemical Name:N-(ethyldiphenylgermylmethyl)benzylamine
CAS No.:132872-05-0
Molecular Formula:C₂₂H₂₅GeN
Molecular Weight:376.037
Hs Code.:

Synonyms:N-(ethyldiphenylgermylmethyl)benzylamine

Suppliers and Price of N-(ethyldiphenylgermylmethyl)benzylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(ethyldiphenylgermylmethyl)benzylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(ethyldiphenylgermylmethyl)benzylamine

There total 1 articles about N-(ethyldiphenylgermylmethyl)benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 132872-04-9
(chloromethyl)ethyldiphenylgermane

: 100-46-9
benzylamine

: 132872-05-0
N-(ethyldiphenylgermylmethyl)benzylamine

Guidance literature:: In neat (no solvent); (dry N2); stirring mixt. of Ge-compd. and large excess of PhCH2NH2 at 80°C (18 h); addn. of aq. 2 M NaOH, sepn. of the org. layer, extn. of the aq. layer (Et2O, three times), drying the combined org. layer and exts. (Na2SO4), evapn., chromy. (silica gel, hexane/ethyl acetate 5:1); mass spectroscopic examn.;
DOI:10.1246/bcsj.67.160

Reference yield: 91.0%

: 132872-05-0
N-(ethyldiphenylgermylmethyl)benzylamine

: 25468-43-3
N-benzyl-N-pentylamine

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; molar ratio amine : BuLi = 1.3:2.9, addn. of BuLi in hexane to a soln. of Ge-compd. in THF at 0°C, stirred at 0°C for 1 h; quenched with water, sepn. of organic layer, dried (Na2SO4), column chromy. (silica gel);