Ethyldiphenylgermane

Base Information

Chemical Name:Ethyldiphenylgermane
CAS No.:72454-22-9
Molecular Formula:C₁₄H₁₆Ge
Molecular Weight:256.871
Hs Code.:

Synonyms:Ethyldiphenylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyldiphenylgermane

Chemical Property:

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Technology Process of Ethyldiphenylgermane

There total 11 articles about Ethyldiphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 132872-05-0
N-(ethyldiphenylgermylmethyl)benzylamine

: 25468-43-3
N-benzyl-N-pentylamine

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; molar ratio amine : BuLi = 1.3:2.9, addn. of BuLi in hexane to a soln. of Ge-compd. in THF at 0°C, stirred at 0°C for 1 h; quenched with water, sepn. of organic layer, dried (Na2SO4), column chromy. (silica gel);

Reference yield: 91.0%

: 109-72-8,29786-93-4
n-butyllithium

: 132872-05-0
N-(ethyldiphenylgermylmethyl)benzylamine

: 25468-43-3
N-benzyl-N-pentylamine

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: In tetrahydrofuran; hexane; at 0 ℃; for 1h;

Reference yield: 68.0%

: 132872-05-0
N-(ethyldiphenylgermylmethyl)benzylamine

: 4111-54-0
lithium diisopropyl amide

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: With water; In tetrahydrofuran; hexane; (dry N2); addn. large excess of LDA in hexane to Ge-compd. in THF at 0°C, stirring at 0°C (1 h), addn. of distd. H2O; extn. (Et2O), drying combined exts. (Na2SO4), evapn., chromy. (silica gel, benzene/ethyl acetate);
DOI:10.1246/bcsj.67.160