3-Chlorobibenzyl

Base Information

• Chemical Name: 3-Chlorobibenzyl
• CAS No.: 34176-92-6
• Molecular Formula: C14H13Cl
• Molecular Weight: 216.71
• Hs Code.: 2903999090
• Mol file: 34176-92-6.mol

Synonyms:3-Chlor-benzylisothiocyanat;Benzene,1-chloro-3-(isothiocyanatomethyl);1-m-Chlorphenyl-2-phenylaethan;m-Chlorobenzyl isothiocyanate;3-Chlor-dibenzyl;4-Chlor-1,2-diphenylethan;Isothiocyanic acid,3-chlorobenzyl ester;3-Chlorobibenzyl;3-Chlor-bibenzyl;3-chlorobenzylisothiocyanate;ISOTHIOCYANIC ACID,m-CHLOROBENZYL ESTER;

Chemical Property of 3-Chlorobibenzyl

Chemical Property:

• Vapor Pressure: 0.00372mmHg at 25°C
• Boiling Point: 289.9°C at 760 mmHg
• Flash Point: 117.4°C
• PSA: 0.00000
• Density: 1.111g/cm³
• LogP: 4.12520

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Chlorobibenzyl

There total 9 articles about 3-Chlorobibenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H13ClO4 (84648-15-7) → styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3-chloro-bibenzyl (34176-92-6) + 2-phenylethyl chloride (622-24-2) + 3-Chloro-benzoic acid phenethyl ester (84648-22-6) + 1,3-Dichlorobenzene (541-73-1)

Guidance literature:

In various solvent(s); at 100 ℃; Mechanism; CIDNP, thermolyse;

DOI:10.1021/jo00155a006

Reference yield:

C16H13ClO4 (84648-15-7) → styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + ethylbenzene (100-41-4,27536-89-6) + 3-chloro-bibenzyl (34176-92-6) + 3-Chloro-benzoic acid phenethyl ester (84648-22-6) + chlorobenzene (108-90-7)

Guidance literature:

In cyclohexanone; at 100 ℃; Mechanism; CIDNP, thermolyse;

DOI:10.1021/jo00155a006

Reference yield:

di-t-butyldiazene (927-83-3) + 1-chloro-3-methylbenzene (108-41-8) + toluene (108-88-3,15644-74-3,16713-13-6) → 1-Chlor-3-neopentyl-benzol (24788-10-1) + (2,2-dimethyl-1-propyl)benzene (1007-26-7) + 1,2-bis(3-chlorophenyl)ethane (19829-55-1) + 3-chloro-bibenzyl (34176-92-6) + 1,1'-(1,2-ethanediyl)bisbenzene (103-29-7)

Guidance literature:

at 80 ℃; for 20h; Product distribution; Irradiation;

DOI:10.1021/ja00374a031

upstream raw materials:

(E)-3-chlorostilbene

1-chloro-3-(2-chloroethyl)benzene

benzene

1-(m-Chlorphenyl)-3-phenyl-propanon-⁽²⁾

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