(O-methyl phenylphosphinite)pentacarbonyltungsten

Base Information

Chemical Name:(O-methyl phenylphosphinite)pentacarbonyltungsten
CAS No.:82265-66-5
Molecular Formula:C₁₂H₉O₆PW
Molecular Weight:464.024
Hs Code.:

Synonyms:(O-methyl phenylphosphinite)pentacarbonyltungsten

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Chemical Property of (O-methyl phenylphosphinite)pentacarbonyltungsten

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Technology Process of (O-methyl phenylphosphinite)pentacarbonyltungsten

There total 4 articles about (O-methyl phenylphosphinite)pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 67-56-1
methanol

: 852242-57-0
3-phenyl-3H-3-benzophosphenine pentacarbonyltungsten⁽⁰⁾

: 82265-66-5
(O-methyl phenylphosphinite)pentacarbonyltungsten

Guidance literature:: In methanol; complex C10H8P(C6H5)W(CO)5 reacted with methanol at 75-80°C;
DOI:10.1021/ja050817y

Reference yield: 87.0%

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 82265-66-5
(O-methyl phenylphosphinite)pentacarbonyltungsten

Guidance literature:: With methanol; In toluene; Cr complex heated at 150°C for 16 h under Ar in sealed tube withMeOH and toluene; evapn., chromy. (SiO2, hexane-toluene); elem. anal.;

Reference yield: 76.0%

: 67-56-1
methanol

: [(CH₃)2(CH₃O₂C)2C₆H₂P(C₆H₅)W(CO)5]

: 82265-66-5
(O-methyl phenylphosphinite)pentacarbonyltungsten

Guidance literature:: With CuCl; 1-phenyl-3,4-dimethylphospholene; In chloroform; (N2); complex, phospholene and CuCl in CHCl3 stirred at room temp., 1 equiv. benzaldehyde or isobutyraldehyde added; after 5 min, MeOH added, stirred for 45 min; evapd., chromd. (SiO2, pentane/toluene);
DOI:10.1016/S0022-328X(00)00601-X