Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn

Base Information

Chemical Name:Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn
CAS No.:4104-91-0
Molecular Formula:C₂₂H₂₀Sn
Molecular Weight:403.111
Hs Code.:

Triphenyl-butin-<sup>(1)</sup>-yl-<sup>(3)</sup>-zinn

Synonyms:Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn

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Chemical Property of Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn

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Technology Process of Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn

There total 20 articles about Triphenyl-butin-⁽¹⁾-yl-⁽³⁾-zinn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 689-97-4
3-buten-1-yne

: 892-20-6
triphenylstannane

: 4104-92-1,4104-91-0
Triphenyl-butadien-(1,2)-yl-⁽¹⁾-zinn

Guidance literature:: In tetrahydrofuran; 70°C, 3 h, molar ratio = 5:1, in presence of azobisisobutyronitrile;;
DOI:10.1016/S0022-328X(00)93515-0

Reference yield: 80.0%

: 16169-82-7
(+/-)-3-acetyloxy-1-butyne

: 79061-17-9
lithium bis(trimethylstannyl)cuprate

: 4104-92-1,4104-91-0
Triphenyl-butadien-(1,2)-yl-⁽¹⁾-zinn

Guidance literature:: In tetrahydrofuran; under N2, to stannylcopper(I) reagent added at -60°C propargyliccompd., stirred for 1 h at -30°C, poured into satd. soln. of NH4Cl in water contg. NaCN; extd. with ether/pentane, washed with water, dried with MgSO4, evapd. in vac., chromd. (Al2O3-5% H2O/n-hexane) or crystd. from methanol;
DOI:10.1016/S0022-328X(00)98533-4

Reference yield: 80.0%

: 79061-17-9
lithium bis(trimethylstannyl)cuprate

: 59967-06-5
1-methylprop-2-ynyl methanesulfonate

: 4104-92-1,4104-91-0
Triphenyl-butadien-(1,2)-yl-⁽¹⁾-zinn

Guidance literature:: In tetrahydrofuran; under N2, to stannylcopper(I) reagent added at -60°C propargyliccompd., stirred for 1 h at -60°C, poured into satd. soln. of NH4Cl in water contg. NaCN; extd. with ether/pentane, washed with water, dried with MgSO4, evapd. in vac., chromd. (Al2O3-5% H2O/n-hexane) or crystd. from methanol;
DOI:10.1016/S0022-328X(00)98533-4