4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

Base Information

Chemical Name:4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt
CAS No.:1313613-20-5
Molecular Formula:CH₄O₃S*C₁₈H₂₅N₃O₄
Molecular Weight:443.521
Hs Code.:

Synonyms:4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

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Chemical Property of 4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

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Technology Process of 4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

There total 7 articles about 4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1117893-61-4
R-(2-oxo-3-((4-(3-oxo-morpholinyl)phenyl)oxazolidin-5-yl))methylmethanesulfonate

: 75-64-9
tert-butylamine

: 1313613-20-5
4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 24h;

Reference yield:

: 446292-04-2
4-(4-nitrophenyl)-3-morpholinone

: 1313613-20-5
4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / 5% Pd(II)/C(eggshell) / water; tetrahydrofuran / 6.5 h / 70 °C / 2250.23 Torr

2: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C

3: lithium tert-butoxide / tetrahydrofuran / 24 h / 20 °C

4: triethylamine / dichloromethane / 4 h / 20 °C

5: N,N-dimethyl-formamide / 24 h / 80 °C

With hydrogen; sodium hydrogencarbonate; triethylamine; lithium tert-butoxide; 5% Pd(II)/C(eggshell); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 122-98-5
2-Anilinoethanol

: 1313613-20-5
4-(4-((S)-5-(tert-butylaminomethyl)-2-oxooxazolidin-3-yl)phenyl)morpholin-3-one methanesulfonic salt

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / isopropyl alcohol / 0 - 40 °C / pH 7 - 8

2: nitric acid; sulfuric acid / 1 h / -10 °C

3: hydrogen / 5% Pd(II)/C(eggshell) / water; tetrahydrofuran / 6.5 h / 70 °C / 2250.23 Torr

4: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C

5: lithium tert-butoxide / tetrahydrofuran / 24 h / 20 °C

6: triethylamine / dichloromethane / 4 h / 20 °C

7: N,N-dimethyl-formamide / 24 h / 80 °C

With sulfuric acid; hydrogen; nitric acid; sodium hydrogencarbonate; triethylamine; sodium hydroxide; lithium tert-butoxide; 5% Pd(II)/C(eggshell); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetone;