N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

Base Information

Chemical Name:N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide
CAS No.:478533-65-2
Molecular Formula:C₁₅H₁₅ClN₂O₂S
Molecular Weight:322.815
Hs Code.:

N'<sup>1</sup>-[(4-chlorophenyl)methylene]-N<sup>1</sup>,4-dimethyl-1-benzenesulfonohydrazide

Synonyms:N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

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Technology Process of N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

There total 3 articles about N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

: 121-45-9
phosphorous acid trimethyl ester

: 478533-65-2
N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

Guidance literature:: With diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 10.1667h;
DOI:10.1080/00397911.2013.786088

Reference yield:

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

: 478533-65-2
N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

Guidance literature:: With potassium carbonate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ol403447g

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 478533-65-2
N'¹-[(4-chlorophenyl)methylene]-N¹,4-dimethyl-1-benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: triphenylphosphine; potassium carbonate / tetrahydrofuran / 2 h / 20 °C

With potassium carbonate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/ol403447g