3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester

Base Information

Chemical Name:3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester
CAS No.:1093192-05-2
Molecular Formula:C₁₄H₂₂N₂O₂
Molecular Weight:250.341
Hs Code.:
Mol file:1093192-05-2.mol

Synonyms:(S)-methyl 3-amino-3-methyl-2-(((S)-1-phenylethyl)amino)butanoate

Suppliers and Price of 3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester

There total 3 articles about 3-aMino-3-Methyl-2(S)-(1(S)-phenylethylaMino)butyric acid Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 1093192-04-1
(S)-methyl 3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoate

: 1093192-05-2
(S)-methyl 3-amino-3-methyl-2-(((S)-1-phenylethyl)amino)butanoate

Guidance literature:: With 4 A molecular sieve; acetic acid; zinc; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

Reference yield:

: 1093192-03-0
(S)-3-methyl-3-nitro-2-(((S)-1-phenylethyl)amino)butanoic acid

: 1093192-05-2
(S)-methyl 3-amino-3-methyl-2-(((S)-1-phenylethyl)amino)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

1.2: 13.25 h / 0 - 20 °C / Inert atmosphere

1.3: pH 7 - 8

2.1: acetic acid / tetrahydrofuran / 3.33 h / 0 °C / Molecular sieve 4?; Inert atmosphere

2.2: 18 h / 0 - 20 °C

With caesium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1093192-05-2
(S)-methyl 3-amino-3-methyl-2-(((S)-1-phenylethyl)amino)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / water / 45 °C / Inert atmosphere

1.2: 3 h / 35 - 46 °C / Inert atmosphere

1.3: 12 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

2.2: 13.25 h / 0 - 20 °C / Inert atmosphere

2.3: pH 7 - 8

3.1: acetic acid / tetrahydrofuran / 3.33 h / 0 °C / Molecular sieve 4?; Inert atmosphere

3.2: 18 h / 0 - 20 °C

With caesium carbonate; acetic acid; potassium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;