C₁₃H₁₉NOSi

Base Information

• Chemical Name: C₁₃H₁₉NOSi
• CAS No.: 138761-36-1
• Molecular Formula: C₁₃H₁₉NOSi
• Molecular Weight: 233.385
• Mol file: 138761-36-1.mol

Synonyms:C₁₃H₁₉NOSi

Chemical Property of C₁₃H₁₉NOSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₉NOSi

There total 2 articles about C₁₃H₁₉NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-benzalacetone (1896-62-4) → C13H19NOSi (138761-36-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₂OH*HCl, NaOH / ethanol; H₂O / 1 h / Heating

2: Et₃N / tetrahydrofuran / 1 h / Ambient temperature

With sodium hydroxide; hydroxylamine hydrochloride; triethylamine; In tetrahydrofuran; ethanol; water;

DOI:10.1055/s-1991-28422

Reference yield:

chloro-trimethyl-silane (75-77-4) + [((E)-4-phenylbut-3-en-2-ylidene)amino]hydroxide (61210-87-5) → C13H19NOSi (138761-36-1)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1055/s-1991-28422

Reference yield: 65.0%

C13H19NOSi (138761-36-1) → (E)-N-styrylacetamide (1722-84-5,18793-45-8,18793-44-7)

Guidance literature:

silver hexafluoroantimonate; antimonypentachloride; In dichloromethane; acetonitrile; at 40 ℃; for 6h;

DOI:10.1246/cl.1991.1653

upstream raw materials:

chloro-trimethyl-silane

[((E)-4-phenylbut-3-en-2-ylidene)amino]hydroxide

(E)-benzalacetone

Downstream raw materials:

(E)-N-styrylacetamide