C₄₂H₄₇F₃N₆O₉S

Base Information

Chemical Name:C₄₂H₄₇F₃N₆O₉S
CAS No.:1315326-72-7
Molecular Formula:C₄₂H₄₇F₃N₆O₉S
Molecular Weight:868.931
Hs Code.:

C<sub>42</sub>H<sub>47</sub>F<sub>3</sub>N<sub>6</sub>O<sub>9</sub>S

Synonyms:C₄₂H₄₇F₃N₆O₉S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₂H₄₇F₃N₆O₉S

Chemical Property:

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Technology Process of C₄₂H₄₇F₃N₆O₉S

There total 9 articles about C₄₂H₄₇F₃N₆O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62965-35-9
N-tert-butyloxycarbonyl-L-tert-leucine

: 1315326-71-6
(2S,4R)-N-((1R,2S)-1-(cyclopropylsulfonylcarbamoyl)-2-vinylcyclopropyl)-4-(2-(4-(trifluoromethyl)phenyl)benzofuro[3,2-d]pyrimidin-4-yloxy)pyrrolidine-2-carboxamide hydrochloride

: 1315326-72-7
C₄₂H₄₇F₃N₆O₉S

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; HATU; In dichloromethane; at 20 ℃;

Reference yield:

: 54802-10-7
3-aminobenzofuran-2-carboxamide

: 1315326-72-7
C₄₂H₄₇F₃N₆O₉S

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / tetrahydrofuran / 0 - 20 °C

2.1: potassium tert-butylate / water; tert-butyl alcohol / 70 °C

2.2: pH ~ 2

3.1: trichlorophosphate / 1,4-dioxane / 6.5 h / 0 - 110 °C

3.2: pH 8

4.1: sodium t-butanolate / dimethyl sulfoxide / 2 h / 10 - 20 °C

4.2: 1 h / 20 °C

4.3: pH ~ 3

5.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 3 h / 20 °C

6.1: thionyl chloride / methanol / 5 h / 0 - 45 °C

7.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

With 4-methyl-morpholine; pyridine; thionyl chloride; potassium tert-butylate; benzotriazol-1-ol; HATU; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 611-20-1
salicylonitrile

: 1315326-72-7
C₄₂H₄₇F₃N₆O₉S

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 3 h / 80 °C

2.1: potassium tert-butylate / tert-butyl alcohol / 3 h / 80 °C

3.1: pyridine / tetrahydrofuran / 0 - 20 °C

4.1: potassium tert-butylate / water; tert-butyl alcohol / 70 °C

4.2: pH ~ 2

5.1: trichlorophosphate / 1,4-dioxane / 6.5 h / 0 - 110 °C

5.2: pH 8

6.1: sodium t-butanolate / dimethyl sulfoxide / 2 h / 10 - 20 °C

6.2: 1 h / 20 °C

6.3: pH ~ 3

7.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 3 h / 20 °C

8.1: thionyl chloride / methanol / 5 h / 0 - 45 °C

9.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

With 4-methyl-morpholine; pyridine; thionyl chloride; potassium tert-butylate; potassium carbonate; benzotriazol-1-ol; HATU; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;