2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

Base Information

Chemical Name:2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid
CAS No.:222416-36-6
Molecular Formula:C₂₃H₂₀O₆
Molecular Weight:392.408
Hs Code.:

Synonyms:2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

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Chemical Property of 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

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Technology Process of 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

There total 7 articles about 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83-56-7
1,5-dihydroxynaphthalene

: 222416-36-6
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 40 percent / K₂CO₃ / acetone / 10 h / Ambient temperature

4: 20 percent / Pd(OAc)2, PPh₃, Et₃N / dimethylformamide / 18 h / 100 °C

5: KOH/MeOH / 1 h / Heating

With methanol; palladium diacetate; potassium hydroxide; potassium carbonate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919908085807

Reference yield:

: 3588-80-5
5-methoxynaphthalen-1-ol

: 222416-36-6
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

Guidance literature:: Multi-step reaction with 4 steps

3: 20 percent / Pd(OAc)2, PPh₃, Et₃N / dimethylformamide / 18 h / 100 °C

4: KOH/MeOH / 1 h / Heating

With methanol; palladium diacetate; potassium hydroxide; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1080/00397919908085807

Reference yield:

: 10075-63-5
1,5-dimethoxynaphthalene

: 222416-36-6
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid

Guidance literature:: Multi-step reaction with 5 steps

4: 20 percent / Pd(OAc)2, PPh₃, Et₃N / dimethylformamide / 18 h / 100 °C

5: KOH/MeOH / 1 h / Heating

With methanol; palladium diacetate; potassium hydroxide; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1080/00397919908085807