2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

Base Information

Chemical Name:2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester
CAS No.:222416-33-3
Molecular Formula:C₂₅H₂₄O₆
Molecular Weight:420.462
Hs Code.:

Synonyms:2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

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Chemical Property of 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

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Technology Process of 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

There total 5 articles about 2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 617-52-7
Dimethyl itakonate

: 107941-39-9
2-bromo-5-methoxy-1-(phenylmethoxy)naphthalene

: 222416-33-3
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 18h;
DOI:10.1080/00397919908085807

Reference yield:

: 83-56-7
1,5-dihydroxynaphthalene

: 222416-33-3
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / K₂CO₃ / acetone / 10 h / Ambient temperature

4: 65 percent / Pd(OAc)2, PPh₃, Et₃N / dimethylformamide / 18 h / 100 °C

With palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919908085807

Reference yield:

: 3588-80-5
5-methoxynaphthalen-1-ol

: 222416-33-3
2-[1-(1-Benzyloxy-5-methoxy-naphthalen-2-yl)-meth-(E)-ylidene]-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

3: 65 percent / Pd(OAc)2, PPh₃, Et₃N / dimethylformamide / 18 h / 100 °C

With palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1080/00397919908085807