6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

Base Information

Chemical Name:6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide
CAS No.:428879-80-5
Molecular Formula:C₃₂H₅₀N₄O₂
Molecular Weight:522.775
Hs Code.:

Synonyms:6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

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Chemical Property of 6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

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Technology Process of 6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

There total 1 articles about 6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 428879-79-2
[5-(benzyl-{6-[benzyl-(6-benzyloxycarbonylaminohexanoyl)amino]hexyl}carbamoyl)pentyl]carbamic acid benzyl ester

: 428879-80-5
6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

Guidance literature:: With acetic acid; trifluoroacetic acid; for 2h;
DOI:10.1021/jm011067f

Reference yield: 40.0%

: 428879-80-5
6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

: 428879-81-6
N¹-{6-[(6-aminohexyl)benzylamino]hexyl}-N¹-benzylhexane-1,6-diamine

Guidance literature:: With dimethylsulfide borane complex; In diethylene glycol dimethyl ether; at 120 ℃; for 10h;
DOI:10.1021/jm011067f

Reference yield:

: 428879-80-5
6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

: 851229-31-7
(3-aminopropyl)-[6-(benzyl-{6-[benzyl-(6-tert-butoxycarbonylaminohexyl)amino]hexyl}amino)hexyl]carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / 10 M BH₃*MeSMe / bis-(2-methoxy-ethyl) ether / 10 h / 120 °C

2: 35 percent / methanol / 3 h / 0 °C

3: 100 percent / CHCl₃

4: 70 percent / H₂; 40percent aq. NaOH / Raney Ni / ethanol / 6 h / 20 °C / 775.74 Torr

With dimethylsulfide borane complex; hydrogen; nickel; In methanol; ethanol; chloroform; diethylene glycol dimethyl ether;
DOI:10.1021/jm011067f