3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

Base Information

Chemical Name:3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile
CAS No.:428879-82-7
Molecular Formula:C₃₅H₅₇N₅
Molecular Weight:547.871
Hs Code.:

Synonyms:3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

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Chemical Property of 3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

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Technology Process of 3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

There total 3 articles about 3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 107-13-1,25014-41-9
acrylonitrile

: 428879-81-6
N¹-{6-[(6-aminohexyl)benzylamino]hexyl}-N¹-benzylhexane-1,6-diamine

: 428879-82-7
3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

: 428879-83-8
3-{6-[benzyl-(6-{benzyl-[6-(2-cyanoethylamino)hexyl]amino}hexyl)amino]hexylamino}propionitrile

Guidance literature:: In methanol; at 0 ℃; for 3h;
DOI:10.1021/jm011067f

Reference yield:

: 428879-80-5
6-aminohexanoic acid {6-[(6-aminohexanoyl)benzylamino]hexyl}benzylamide

: 428879-82-7
3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / 10 M BH₃*MeSMe / bis-(2-methoxy-ethyl) ether / 10 h / 120 °C

2: 35 percent / methanol / 3 h / 0 °C

With dimethylsulfide borane complex; In methanol; diethylene glycol dimethyl ether;
DOI:10.1021/jm011067f

Reference yield:

: 428879-79-2
[5-(benzyl-{6-[benzyl-(6-benzyloxycarbonylaminohexanoyl)amino]hexyl}carbamoyl)pentyl]carbamic acid benzyl ester

: 428879-82-7
3-[6-({6-[(6-aminohexyl)benzylamino]hexyl}benzylamino)hexylamino]propionitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 30percent HBr; AcOH; CF₃COOH / 2 h

2: 40 percent / 10 M BH₃*MeSMe / bis-(2-methoxy-ethyl) ether / 10 h / 120 °C

3: 35 percent / methanol / 3 h / 0 °C

With dimethylsulfide borane complex; acetic acid; trifluoroacetic acid; In methanol; diethylene glycol dimethyl ether;
DOI:10.1021/jm011067f