p,p'-bis-(trifluoromethyl)azoxybenzene

Base Information

Chemical Name:p,p'-bis-(trifluoromethyl)azoxybenzene
CAS No.:34913-34-3
Molecular Formula:C₁₄H₈F₆N₂O
Molecular Weight:334.221
Hs Code.:

Synonyms:p,p'-bis-(trifluoromethyl)azoxybenzene

Suppliers and Price of p,p'-bis-(trifluoromethyl)azoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of p,p'-bis-(trifluoromethyl)azoxybenzene

Chemical Property:

Boiling Point:349.8±52.0 °C(Predicted)
Density:1.38±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of p,p'-bis-(trifluoromethyl)azoxybenzene

There total 8 articles about p,p'-bis-(trifluoromethyl)azoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 455-14-1
4-trifluoromethylphenylamine

: 34913-34-3
p,p'-bis-(trifluoromethyl)azoxybenzene

Guidance literature:: With fluorosulfonyl fluoride; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2021.153457

Reference yield: 86.0%

: 402-54-0
p-nitrobenzotrifluoride

: 34913-34-3
p,p'-bis-(trifluoromethyl)azoxybenzene

Guidance literature:: With ammonia; lithium perchlorate; In acetonitrile; at 20 ℃; for 4h; chemoselective reaction; Electrolysis;
DOI:10.1039/d1ob00077b

Reference yield: 18.0%

: oxo(N-4-trifluoromethylphenylhydroxylamido-O,N)(pyridine-2,6-dicarboxylato)(hexamethylphosphortriamide)molybdenum(VI)

: 586-96-9
Nitrosobenzene

: oxo-(N-(C₆H₅)hydroxylamido-O,N)(pyridine-2,6-dicarboxylato)(hexamethylphosphoramide)molybdenum(VI)

: 328945-86-4,68866-26-2
dioxo-(pyridine-2,6-dicarboxylato)(hexamethylphosphoramide)molybdenum(VI)

: 64857-62-1
p-(trifluormethyl)azoxybenzene

: 34913-34-3
p,p'-bis-(trifluoromethyl)azoxybenzene

: 495-48-7,55599-32-1
azoxybenzene

Guidance literature:: In 1,4-dioxane; Mo-complex and nitrosobenzene dissolved in dioxane, mixt. refluxed (6 h); further product: 30% p'-(trifluormethyl)azoxybenzene; evapn. (rotary evaporator), residue washed (petroleum ether), filtered; also contains 24% of starting Mo-complex;