[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Base Information

Chemical Name:[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester
CAS No.:1369205-95-7
Molecular Formula:C₁₉H₂₃NO₄S
Molecular Weight:361.462
Hs Code.:

Synonyms:[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Suppliers and Price of [2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

There total 10 articles about [2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1369205-94-6
toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

: 1369205-95-7
[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester; With O,O'-dibenzoyl-L-tartaric acid; In ethyl acetate; at 10 - 20 ℃; for 5h; Cooling;

With ammonium hydroxide; In dichloromethane; water; at 20 - 25 ℃; for 1h;

Reference yield: 85.0%

: 1369205-97-9
dibenzoyl-L-tartaric acid [2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

: 1369205-95-7
[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: With ammonium hydroxide; In dichloromethane; at 20 - 25 ℃; for 1h;

Reference yield:

: 13103-80-5
1-(3-hydroxyphenyl)propan-1-one

: 1369205-95-7
[2S]-toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / isopropyl alcohol; water / 16 h / Reflux

2.1: potassium carbonate / dichloromethane / 1 h / 30 - 35 °C

3.1: O,O'-dibenzoyl-L-tartaric acid / ethyl acetate / 5 h / 10 - 20 °C / Cooling

3.2: 1 h / 20 - 25 °C

With hydrogenchloride; potassium carbonate; O,O'-dibenzoyl-L-tartaric acid; In dichloromethane; water; ethyl acetate; isopropyl alcohol;