pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride

Base Information

• Chemical Name: pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride
• CAS No.: 937030-04-1
• Molecular Formula: C₁₃H₁₁N₂*Cl
• Molecular Weight: 230.697
• Mol file: 937030-04-1.mol

Synonyms:pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride

Chemical Property of pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride

There total 4 articles about pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

pyridine-2-carbaldehyde (1121-60-4) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + aniline (62-53-3) → pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride (937030-04-1)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 0.25h;

DOI:10.1021/ol202134n

Reference yield: 86.0%

C13H12N2O (937030-03-0) → pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride (937030-04-1)

Guidance literature:

With trichlorophosphate; In toluene; for 72h; Reflux;

DOI:10.1021/jo1014933

Reference yield: 78.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (E)-N-(2-pyridylmethylene)aniline (7032-25-9,40468-86-8,88785-71-1) → pyridyl[1,2-a](2-phenylimidazol)-3-ylidene chloride (937030-04-1)

Guidance literature:

formaldehyd; (E)-N-(2-pyridylmethylene)aniline; In toluene; at 20 ℃; for 10h;

With hydrogenchloride; In diethyl ether; toluene; for 10h; Further stages.;

DOI:10.1039/b712901g

upstream raw materials:

formaldehyd

(E)-N-(2-pyridylmethylene)aniline

C₁₃H₁₂N₂O

pyridine-2-carbaldehyde

Downstream raw materials:

methyl 5-(p-bromophenyl)-4-(N-phenyl-N-(2-pyridylmethyl)-amino)-2-propylfuran-3-carboxylate

(Z)-dimethyl 4-(N-(2,3-dimethoxycarbonyl-1-(2-pyridyl)allyl)-N-phenylamino)-5-(2-furyl)furan-2,3-dicarboxylate

(E)-dimethyl 4-(N-(2,3-dimethoxycarbonyl-1-(2-pyridyl)prop-1-enyl)-N-phenylamino)-5-(2-furyl)furan-2,3-dicarboxylate

methyl 5-(p-chlorophenyl)-2-phenethyl-4-(N-phenyl-N-(2-pyridylmethyl)amino)furan-3-carboxylate