N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

Base Information

Chemical Name:N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide
CAS No.:146231-73-4
Molecular Formula:C₄₀H₃₈N₄O₆
Molecular Weight:670.765
Hs Code.:

Synonyms:N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

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Chemical Property of N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

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Technology Process of N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

There total 4 articles about N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 541-41-3
chloroformic acid ethyl ester

: 146231-72-3
N-(4'-Amino-biphenyl-2-yl)-2-{4-[(4'-amino-biphenyl-2-ylcarbamoyl)-methyl]-phenyl}-acetamide

: 146231-73-4
N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

Guidance literature:: With N,N-dimethyl-aniline; In ethanol; for 3h; Heating;
DOI:10.1016/S0040-4039(00)60204-6

Reference yield:

: 21062-19-1
1,4-benzenediacetyl dichloride

: 146231-73-4
N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / benzene / 24 h / Heating

2: 91 percent / H₂ / 10percent Pd/C / dimethylformamide; ethanol / 15 h / 70 °C / 37503 Torr

3: 85 percent / N,N-dimethylaniline / ethanol / 6 h / Heating

With hydrogen; N,N-dimethyl-aniline; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; benzene;

Reference yield:

: 6272-52-2
2-(4-nitrophenyl)aniline

: 146231-73-4
N,N'-bis[(4'-ethyloxycarbonylamino)-2-biphenylyl]-p-phenylenediacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / benzene / 24 h / Heating

2: 91 percent / H₂ / 10percent Pd/C / dimethylformamide; ethanol / 15 h / 70 °C / 37503 Torr

3: 85 percent / N,N-dimethylaniline / ethanol / 6 h / Heating

With hydrogen; N,N-dimethyl-aniline; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; benzene;