Technology Process of 10-Methyl-1,4,7-trioxa-10-azacyclododecan-10-ium
There total 7 articles about 10-Methyl-1,4,7-trioxa-10-azacyclododecan-10-ium which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
formic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaI / acetone / 70 h / Heating
2: 54 percent / Na2CO3 / acetonitrile / 18 h / Heating
3: 85 percent / H2 / Pd/C / acetic acid / 15 h / 60 °C / 2280 Torr
4: 1.) K2CO3, 2.) LiAlH4 / 1.) THF, 2.) RT, 18 h
With
lithium aluminium tetrahydride; hydrogen; sodium carbonate; potassium carbonate; sodium iodide;
palladium on activated charcoal;
In
acetic acid; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / thionyl chloride / pyridine / Ambient temperature
2: NaI / acetone / 70 h / Heating
3: 54 percent / Na2CO3 / acetonitrile / 18 h / Heating
4: 85 percent / H2 / Pd/C / acetic acid / 15 h / 60 °C / 2280 Torr
5: 1.) K2CO3, 2.) LiAlH4 / 1.) THF, 2.) RT, 18 h
With
lithium aluminium tetrahydride; thionyl chloride; hydrogen; sodium carbonate; potassium carbonate; sodium iodide;
palladium on activated charcoal;
In
pyridine; acetic acid; acetone; acetonitrile;
