7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

Base Information

Chemical Name:7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine
CAS No.:505097-26-7
Molecular Formula:C₂₀H₁₇ClN₄
Molecular Weight:348.835
Hs Code.:

Synonyms:7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

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Chemical Property of 7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

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Technology Process of 7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

There total 3 articles about 7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 141-30-0
3,6-dichlorpyridazine

: 505097-16-5
6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

: 505097-26-7
7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

Guidance literature:: With aluminium trichloride; In dichloromethane; at 60 ℃; for 48h;
DOI:10.1016/S0040-4020(02)01352-2

Reference yield:

: 1632-74-2
3,6-dimethylpyridazine

: 505097-26-7
7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyl acetate / 12 h / 70 °C

1.2: 85 percent / sodium bicarbonate / ethanol / 12 h / Heating

2.1: 76 percent / AlCl₃ / CH₂Cl₂ / 48 h / 60 °C

With aluminium trichloride; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(02)01352-2

Reference yield:

: 2632-14-6
4-ethylphenacyl bromide

: 505097-26-7
7-(6-chloro-3-pyridazinyl)-6-(4-ethylphenyl)-2-methylpyrrolo[1,2-b]pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyl acetate / 12 h / 70 °C

1.2: 85 percent / sodium bicarbonate / ethanol / 12 h / Heating

2.1: 76 percent / AlCl₃ / CH₂Cl₂ / 48 h / 60 °C

With aluminium trichloride; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(02)01352-2