diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

Base Information

Chemical Name:diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate
CAS No.:947695-29-6
Molecular Formula:C₂₃H₃₄N₂O₈
Molecular Weight:466.532
Hs Code.:

Synonyms:diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

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Chemical Property of diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

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Technology Process of diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

There total 3 articles about diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128461-65-4
3-(p-methoxybenzyloxy)propanal

: 947695-29-6
diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl azodicarboxylate / acetonitrile / 15 h / 0 °C

2: 4.35 g / benzene / 20 h / 6 °C

With diisopropyl azodicarboxylate; In acetonitrile; benzene; 2: Wittig olefination;
DOI:10.1055/s-2007-966062

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 947695-29-6
diisopropyl 1-{(1S,2E)-4-ethoxy-1-[(4-methoxybenzyl)oxy]methyl-4-oxo-2-butenyl}-1,2-hydrazinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / chloroacetic acid; NaOH; acetic acid / H₂O / 144 h / 20 °C

2: diisopropyl azodicarboxylate / acetonitrile / 15 h / 0 °C

3: 4.35 g / benzene / 20 h / 6 °C

With sodium hydroxide; acetic acid; chloroacetic acid; In water; acetonitrile; benzene; 1: Michael addition / 3: Wittig olefination;
DOI:10.1055/s-2007-966062